HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl Acetate → HCID 53634814, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl Acetate | HCID 8857 | — |
| Reactant | m-Chloroperbenzoic acid | HCID 70297 | — |
| Reactant | HCID 23346412 | HCID 23346412 | — |
| Product | HCID 53634814 | HCID 53634814 | — |
Reaction Steps
4,5-Bis(trifluoromethyl)isatin (283 g., 1 mol.) is suspended in 1 L. of ethyl acetate and treated with m-chloroperbenzoic acid (172 g., 1 mol.), stirred until the oxidation is complete to yield 5,6-bis(trifluoromethyl)-isatoic anhydride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04218464 |
| Source dataset | uspto-grants-1980_08 |
| ORD ID | ord-1339e42314c049619a7aff84a371a113 |
| Source note | uspto-grants-1980_08 |