HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diboron → HCID 23346423, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diboron | HCID 6328200 | — |
| Reactant | HCID 18787738 | HCID 18787738 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 23346423 | HCID 23346423 | — |
Reaction Steps
3,4-Bis(trifluoromethyl)phtalic acid (33 g., 0.11 mol.) in 70 ml. of tetrahydrofuran is refluxed with 450 ml. of 1.0 M diborane in tetrahydrofuran for four hours. Excess diborane is destroyed with water to yield 3,4-bis(trifluoro- methyl)-1,2-benzenedimethanol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04218464 |
| Source dataset | uspto-grants-1980_08 |
| ORD ID | ord-9c417a032c974407846dcfb69957086f |
| Source note | uspto-grants-1980_08 |