HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,6-Diethylaniline → HCID 12546827, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,6-Diethylaniline | HCID 11369 | — |
| Reactant | Propanoyl bromide, 2-bromo- | HCID 79047 | — |
| Product | HCID 12546827 | HCID 12546827 | 80% |
Reaction Steps
Following the procedure described in Example 8A using 2,6-diethylaniline and 2-bromopropionyl bromide the desired intermediate was obtained in 80% yield. Recrystallized from abs. methanol it melted at 197°-199° C. Calcd.: C 54.9, H 6.38, N 4.93, Br 28.1. Found: C 54.8, H 6.19, N 5.02, Br 27.9.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04218477 |
| Source dataset | uspto-grants-1980_08 |
| ORD ID | ord-d5a8bfcacaf943b9aafa2573a6ac46e5 |
| Source note | uspto-grants-1980_08 |