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HRID1856446

反应详情

EQUATION

反应方程式

HRID 1856446 的结构方程式

REACTANTS

反应物

2
结构：O=S(=O)(O)C(F)(F)F
HCID62406

未命名化合物

结构：O=C([O-])[O-].O=C([O-])[O-].O=C([O-])[O-].[La+3].[La+3]
HCID168924

Lanthanum carbonate

C3La2O9

PRODUCTS

生成物

1
结构：O=S(=O)([O-])C(F)(F)F.O=S(=O)([O-])C(F)(F)F.O=S(=O)([O-])C(F)(F)F.[La+3]
HCID2733938

Lanthanum tris(trifluoromethanesulfonate)

C3F9LaO9S3

AUXILIARIES

试剂、催化剂与溶剂

1
结构：O
溶剂HCID962

Water

H2O

PROCEDURE

实验过程

Lanthanum carbonate (15 g.) and trifluoromethanesulfonic acid (22.5 g) are combined as described in Example II. The solution is evaporated at reduced pressure and the residue, dried over sulfuric acid in dessicator. The product obtained, 20.4 g., gave the following analysis: % La 22.06; % S 15.88; % H2O 5.61, indicating an Al:S ratio of 1:3.12.

WORKUP

后处理

  1. customThe solution is evaporated at reduced pressure
  2. dry with materialthe residue, dried over sulfuric acid in dessicator
  3. customThe product obtained
  4. custom, gave the following analysis