HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 23345025, compound → 1-Phenylpiperazine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 23345025 | HCID 23345025 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 1-Phenylpiperazine | HCID 7096 | 95% |
| Product | HCID 23345035 | HCID 23345035 | — |
Reaction Steps
From 10 mmol of 5-[3-(2,3-epoxypropoxy)-4-methoxyphenyl]-2-pyrrolidone and 10 mmol of 1-phenylpiperazine (95% strength), 5-{3-[2-hydroxy-3-(4-phenylpiperazin-1-yl)propoxy]-4-methoxyphenyl }-2-pyrrolidone, m.p. 127°-131° (ethanol) is obtained in 52% yield, analogously to the process of Example 1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04219551 |
| Source dataset | uspto-grants-1980_08 |
| ORD ID | ord-419731da5d3347d692883777be308d75 |
| Source note | uspto-grants-1980_08 |