2-Amino-5-bromopyridine → HCID 19072852, compound

Participants

Reaction Steps

2,6-Dichlorobenzoyl isocyanate (2.16 grams; 0.01 mole) and 5-bromo-2-aminopyridine (1.73 grams; 0.01 mole) were mixed in 50 ml. of ethyl acetate, at room temperature. The reaction mixture was stirred at room temperature for 4 hours, during which the product precipitated. It was separated by filtration and recrystallized from ethanol, m.p. 228°-230° C., yield 2.0 grams. Elemental analysis showed:

Provenance & Evidence