HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 53911873, compound → HCID 54540261, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 53911873 | HCID 53911873 | — |
| Catalyst | Zinc | HCID 23994 | — |
| Solvent | Tetrahydrofuran ethanol | HCID 21873804 | — |
| Product | HCID 54540261 | HCID 54540261 | — |
Reaction Steps
Hexadecanoic acid (4-nitrobutyl)ester was reduced with zinc in EtOH/THF/6 nHCl for 30 minutes at 35°-35°. Work up in the cold via basification with ammonia and extraction with methylene chloride yielded a crude residue. Crystallization from ether furnished off-white crystals, m.p. 59°-61°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04219660 |
| Source dataset | uspto-grants-1980_08 |
| ORD ID | ord-650418e33a3c4bb88c6f6af3c4b56a85 |
| Source note | uspto-grants-1980_08 |