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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1856502Generated: October 29, 2026

Methanol → HCID 54408349, compound

https://huagongshe.com/reaction/1856502

Reaction equation

Participants

RoleNameHCIDCharge
ReactantMethanolHCID 887—
ReactantSodiumHCID 5360545—
ReactantHCID 54297158HCID 54297158—
ProductHCID 54408349HCID 54408349—

Reaction Steps

0.1 Mol of 1-nitro-2-methyl-1,3-butadiene was added to a solution of 0.1 Mol of sodium in methanol and stirred overnight. The reaction mixture was quenched in ice and extracted with methylene chloride. The oily residue was purified via column chromatography. The product was obtained as a yellow liquid.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04219660
Source datasetuspto-grants-1980_08
ORD IDord-e246feaff8524aada86d486c4a2351d3
Source noteuspto-grants-1980_08