HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Nitrobenzoyl chloride → HCID 86737163, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Nitrobenzoyl chloride | HCID 8502 | — |
| Reactant | 3-Methyl-4-nitrobut-2-en-1-ol | HCID 54439127 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | HCID 86737163 | HCID 86737163 | — |
Reaction Steps
To 0.1 Mol of 4-nitro-3-methyl-2-butenol in benzene was added 0.1 Mol of p-Nitrobenzoylchloride and stirred overnight. The benzene was evaporated and the residue was stirred in sat. sodiumbicarbonate solution for 1 hour. The solid was filtered and recrystallized from hexane. An off white crystalline product, mp 63°-66° C., was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04219660 |
| Source dataset | uspto-grants-1980_08 |
| ORD ID | ord-e942335fdd9b4ca3803a9297b9456fe4 |
| Source note | uspto-grants-1980_08 |