Palmitoyl chloride → HCID 86737167, compound

HRID 1856507Notes

Reaction equation

HRID 1856507 reaction equation
[N+:1]([CH2:4][C:5]([CH3:9])=[CH:6][CH2:7][OH:8])([O-:3])=[O:2].[C:10](Cl)(=[O:26])[CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH3:25]>C1C=CC=CC=1>[CH3:9][C:5]([CH2:4][N+:1]([O-:3])=[O:2])=[CH:6][CH2:7][OH:8].[C:10]([O-:26])(=[O:2])[CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH3:25]

Participants

4

Reactant 2

HCID 8206Palmitoyl chlorideHCID 544391273-Methyl-4-nitrobut-2-en-1-ol

Product 1

HCID 86737167HCID 86737167, compound

Reagents, catalysts & solvents 1

HCID 241BenzeneSolvent

Procedure

To 0.1 Mol of 4-nitro-3-methyl-2-butenol in benzene was added 0.1 Mol of palmitoylchloride and stirred overnight. The benzene was evaporated and the residue was taken up in sat. sodiumbicarbonate solution and extracted with ether. The product was crystallized from a 95% ethanol-water solution. Off white crystals, m.p. 30.5°-31.5° C., were obtained.

Workup

  1. customThe benzene was evaporated
  2. extractionextracted with ether
  3. customThe product was crystallized from a 95% ethanol-water solution
  4. customOff white crystals, m.p. 30.5°-31.5° C., were obtained

Sources & evidence

ORD record
ord-c82a249833064c239a13d49cc0c9deb8
Source dataset
uspto-grants-1980_08
Patent number
US04219660

Reaction notes

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