HuagongsheHuagongshe Chemistry Print Report · For research reference only
Palmitoyl chloride → HCID 86737167, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Palmitoyl chloride | HCID 8206 | — |
| Reactant | 3-Methyl-4-nitrobut-2-en-1-ol | HCID 54439127 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | HCID 86737167 | HCID 86737167 | — |
Reaction Steps
To 0.1 Mol of 4-nitro-3-methyl-2-butenol in benzene was added 0.1 Mol of palmitoylchloride and stirred overnight. The benzene was evaporated and the residue was taken up in sat. sodiumbicarbonate solution and extracted with ether. The product was crystallized from a 95% ethanol-water solution. Off white crystals, m.p. 30.5°-31.5° C., were obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04219660 |
| Source dataset | uspto-grants-1980_08 |
| ORD ID | ord-c82a249833064c239a13d49cc0c9deb8 |
| Source note | uspto-grants-1980_08 |