HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzoyl chloride → HCID 86737168, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzoyl chloride | HCID 7412 | — |
| Reactant | 3-Methyl-4-nitrobut-2-en-1-ol | HCID 54439127 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | HCID 86737168 | HCID 86737168 | — |
Reaction Steps
To 0.1 Mol of 4-nitro-3-methyl-2-butenol in benzene was added 0.09 Mol benzoylchloride and stirred overnight. The benzene was evaporated and the residue was stirred with sat. sodiumbicarbonate solution and extracted with ether. The oily product was purified by column chromatography, yielding the product as a slight yellow liquid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04219660 |
| Source dataset | uspto-grants-1980_08 |
| ORD ID | ord-f79df4868c1a45e8a4b8b7fd7579c944 |
| Source note | uspto-grants-1980_08 |