HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chloride → n-Octylsuccinyl dichloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chloride | HCID 312 | — |
| Reactant | Phosphorus pentachloride | HCID 24819 | — |
| Reactant | 2,5-Furandione, dihydro-3-octyl- | HCID 77869 | — |
| Product | n-Octylsuccinyl dichloride | HCID 23345517 | 79.2% |
Reaction Steps
n-Octylsuccinyl dichloride was prepared by reacting n-octylsuccinic anhydride with PCl5 at 105°-110° C. for about four hours. After working the product up 101.3 g of liquid was obtained which had a purity of 84.3% according to chloride content. The corrected yield was 79.2%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04219676 |
| Source dataset | uspto-grants-1980_08 |
| ORD ID | ord-7a5f942dfdec4f5b9ca667a9f9c5440c |
| Source note | uspto-grants-1980_08 |