反应详情

Potassium tert-butoxide (34 g; 0.3 mol) was dissolved in 250 ml of anhydrous tetrahydrofuran (THF) in a round-bottom flask. 5-norbornene-2,3-dicarbonyl chloride (22 g; 0.1 mol) then was slowly added thereto at room temperature, and the reactant was reacted at a temperature of 45° C. for about 12 hours.

1. customat room temperature, and the reactant was reacted at a temperature of 45° C. for about 12 hours