HuagongsheHuagongshe Chemistry Print Report · For research reference only
Bicyclo(2.2.1)hept-5-ene-2-carboxaldehyde → HCID 69823336, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Bicyclo(2.2.1)hept-5-ene-2-carboxaldehyde | HCID 95117 | — |
| Reactant | HCID 178419647 | HCID 178419647 | — |
| Product | HCID 69823336 | HCID 69823336 | — |
Reaction Steps
2-norbornyl magnesiumbromide (200 ml; 0.1 mol in THF) solution was poured into a round-bottom flask and 14 g of 5-norbornene-2-carboxaldehyde (0.11 mol) was slowly dropped thereinto and the reactant was reacted at 45° C. for about 20 hours.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06143465 |
| Source dataset | uspto-grants-2000_11 |
| ORD ID | ord-e142cc8d1db84d92a0b90afd806cede6 |
| Source note | uspto-grants-2000_11 |