HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Bromooctane → HCID 53765542, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Bromooctane | HCID 8140 | — |
| Reactant | 3-Aminophenol | HCID 11568 | — |
| Reactant | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 53765542 | HCID 53765542 | — |
Reaction Steps
A solution of 5.45 g of 3-aminophenol and 11.6 g of 1-bromooctane in 250 ml of dioxane is stirred at 100° C. for 80 hours, the solvent is then evaporated, and the residue is then taken up in toluene/ethyl acetate (10:1) and chromatographed on silica gel, giving N-octylaminophenol as beige crystals, melting point 75° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06143570 |
| Source dataset | uspto-grants-2000_11 |
| ORD ID | ord-ed80d875ccd1439b895cd1642cc2cb04 |
| Source note | uspto-grants-2000_11 |