Triphenylphosphine → HCID 22132375, compound

HRID 1856656Notes

Reaction equation

HRID 1856656 reaction equation
[N:1]([CH2:4][CH:5]1[CH2:10][CH2:9][CH2:8][N:7]([CH:11]2[CH2:16][CH2:15][N:14]([C:17]3[CH:24]=[CH:23][CH:22]=[CH:21][C:18]=3[C:19]#[N:20])[CH2:13][CH2:12]2)[CH2:6]1)=[N+]=[N-].C1(P(C2C=CC=CC=2)C2C=CC=CC=2)C=CC=CC=1>>[NH2:1][CH2:4][CH:5]1[CH2:10][CH2:9][CH2:8][N:7]([CH:11]2[CH2:16][CH2:15][N:14]([C:17]3[CH:24]=[CH:23][CH:22]=[CH:21][C:18]=3[C:19]#[N:20])[CH2:13][CH2:12]2)[CH2:6]1

Participants

3

Reactant 2

HCID 11776TriphenylphosphineHCID 22132362HCID 22132362, compound

Product 1

HCID 22132375HCID 22132375, compound

Procedure

The title compound was prepared from 24 (560 mg, 1.73 mmol) and triphenylphosphine (900 mg, 3.4 mmol) using the procedure described for 13.

Sources & evidence

ORD record
ord-9a1e91efe25e420c965cdee9966a3fb6
Source dataset
uspto-grants-2000_11
Patent number
US06143750

Reaction notes

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