HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,2-Epoxybutane → HCID 419885, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,2-Epoxybutane | HCID 7834 | — |
| Reactant | Cyclohexylamine | HCID 7965 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 419885 | HCID 419885 | 61.3% |
Reaction Steps
To methanol (200 ml) are added 1,2-epoxybutane (72.2 g) and cyclohexylamine (99.2 g), and the mixture is refluxed for 6 hours. The mixture is concentrated under reduced pressure to remove the solvent to give N-(2-hydroxybutyl)-N-cyclohexylamine (105 g) as a colorless oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06143763 |
| Source dataset | uspto-grants-2000_11 |
| ORD ID | ord-38355a80b6c242448ed373ecf5e8779b |
| Source note | uspto-grants-2000_11 |