HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenylacetyl chloride → HCID 22132959, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenylacetyl chloride | HCID 7679 | — |
| Reactant | HCID 86756007 | HCID 86756007 | — |
| Product | HCID 22132959 | HCID 22132959 | 58.5% |
Reaction Steps
40 g (81 mmol) of (2-hydroxy-5-nitrophenyl)-methyltriphenylphosphonium bromide and 21.4 g (162 mmol) of phenylacetyl chloride are treated under the conditions described in step 1 of Example 1. 12 g of product are obtained. Melting point: 100° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06143772 |
| Source dataset | uspto-grants-2000_11 |
| ORD ID | ord-d3de58f062674e1d97d2df6543ff46c9 |
| Source note | uspto-grants-2000_11 |