Ethyl Acetate → HCID 54469756, compound

Participants

Reaction Steps

1.1 g of the product obtained in Stage 6 of Example 1 is introduced, 127 mg of a suspension of sodium hydride at 50% in oil is added and the reaction medium is left under agitation for 15 minutes at ambient temperature. Then 657 mg of the product obtained in Stage 1 of Preparation 1 is added and the reaction medium is left under agitation for 24 hours at ambient temperature, followed by hydrolysis with a saturated solution of ammonium chloride and extraction with ethyl acetate and after chromatography, 880 mg of the expected product (amorphous solid) is obtained.

Provenance & Evidence