HRID1857097

反应详情

EQUATION

反应方程式

HRID 1857097 的结构方程式

CONDITIONS

反应条件

温度
180 °C

PROCEDURE

实验过程

4-Chloro-6,7-dimethoxyquinoline (75 mg) and 6-methoxy-2-naphthol (174 mg) obtained in Example 1 were mixed and stirred at 180° C. for 30 minutes, and the reaction mixture was then purified by thin layer chromatography on silica gel (eluting with hexane/acetone (2/1)) to obtain 71 mg of the title compound (yield: 59%).

WORKUP

后处理

  1. customthe reaction mixture was then purified by thin layer chromatography on silica gel (eluting with hexane/acetone (2/1))