HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1857102Generated: November 2, 2026
3,4-Dimethoxyphenol → HCID 9927943, compound
https://huagongshe.com/reaction/1857102
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 3,4-Dimethoxyphenol | HCID 16251 | — |
| Reactant | 4-Chloro-6,7-dimethoxyquinoline | HCID 459610 | — |
| Product | HCID 9927943 | HCID 9927943 | 19% |
Reaction Steps
4-Chloro-6,7-dimethoxyquinoline (90 mg) and commercially available 3,4-dimethoxyphenol (187 mg) were mixed and stirred at 180° C. for 30 minutes, and the mixture was then purified by column chromatography on silica gel eluting with hexane/acetone to obtain 26 mg of the title compound (yield: 19%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US06143764 |
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| Source dataset | uspto-grants-2000_11 |
|---|
| ORD ID | ord-e7b58e3f191f4e1ba42c8d638753a97f |
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| Source note | uspto-grants-2000_11 |
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