Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1857113Generated: October 28, 2026

3-Methoxybenzenethiol → HCID 22132683, compound

https://huagongshe.com/reaction/1857113

Reaction equation

Participants

RoleNameHCIDCharge
Reactant3-MethoxybenzenethiolHCID 84989—
Reactant4-Chloro-6,7-dimethoxyquinolineHCID 459610—
ProductHCID 22132683HCID 22132683100%

Reaction Conditions

Temperature180 °C

Reaction Steps

4-Chloro-6,7-dimethoxyquinoline (50 mg) and commercially available 3-methoxybenzenethiol (77 mg) were mixed and stirred at 180° C. for 30 seconds. Purification was carried out in the same manner as described in Example 18 to obtain 72 mg of the title compound (yield: 100%).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06143764
Source datasetuspto-grants-2000_11
ORD IDord-a80957b74fba4db7af0ea9dacbaa494f
Source noteuspto-grants-2000_11