HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1857114Generated: November 3, 2026
4-Methoxybenzenethiol → HCID 22132769, compound
https://huagongshe.com/reaction/1857114
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 4-Methoxybenzenethiol | HCID 12765 | — |
| Reactant | 4-Chloro-6,7-dimethoxyquinoline | HCID 459610 | — |
| Product | HCID 22132769 | HCID 22132769 | 109.3% |
Reaction Steps
4-Chloro-6,7-dimethoxyquinoline (50 mg) and commercially available 4-methoxybenzenethiol (63 mg) were mixed and stirred at 150° C. for 5 minutes. Purification was carried out in the same manner as described in Example 18, and further crystallization with chloroform gave 80 mg of the title compound (yield: 100%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US06143764 |
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| Source dataset | uspto-grants-2000_11 |
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| ORD ID | ord-c18294d86b614146a6f0d0905ad0565e |
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| Source note | uspto-grants-2000_11 |
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