HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1857121Generated: November 1, 2026
Methanone, [4-(1,1-dimethylethyl)phenyl](4-hydroxyphenyl)- → HCID 9932979, compound
https://huagongshe.com/reaction/1857121
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Methanone, [4-(1,1-dimethylethyl)phenyl](4-hydroxyphenyl)- | HCID 108659 | — |
| Reactant | 4-Chloro-6,7-dimethoxyquinoline | HCID 459610 | — |
| Product | HCID 9932979 | HCID 9932979 | 11% |
Reaction Steps
4-Chloro-6,7-dimethoxyquinoline (341 mg) and 4-t-butylphenyl 4-hydroxyphenyl ketone (775 mg) obtained in Example 30 were mixed and stirred at 150° C. for 15 minutes. The reaction mixture was then purified by column chromatography on silica gel eluting with hexane/acetone to obtain 72 mg of the title compound (yield: 11%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US06143764 |
|---|
| Source dataset | uspto-grants-2000_11 |
|---|
| ORD ID | ord-1712283d17b74cf6a2b4cb6beaf76686 |
|---|
| Source note | uspto-grants-2000_11 |
|---|
