HuagongsheHuagongshe Chemistry Print Report · For research reference only
(4-methoxyphenyl)(naphthalen-2-yl)methanone → HCID 15640646, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (4-methoxyphenyl)(naphthalen-2-yl)methanone | HCID 267822 | — |
| Reactant | Sodium methanethiolate | HCID 4378561 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 15640646 | HCID 15640646 | 86% |
Reaction Steps
4-Methoxyphenyl 2-naphthyl ketone (735 mg) obtained in Example 35 was dissolved in N,N-dimethylformamide (20 ml), sodium thiomethoxide (491 mg) was added, and the admixture was refluxed under argon for 5 hours. The reaction mixture was treated in the same manner as described in Example 33 to obtain 595 mg of the title compound (yield: 86%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06143764 |
| Source dataset | uspto-grants-2000_11 |
| ORD ID | ord-0b6e6f7945f146d7a0d08b4d122512c5 |
| Source note | uspto-grants-2000_11 |