HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1857127Generated: November 3, 2026
4-Chloro-6,7-dimethoxyquinoline → HCID 22132807, compound
https://huagongshe.com/reaction/1857127
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 4-Chloro-6,7-dimethoxyquinoline | HCID 459610 | — |
| Reactant | 4-(Thiophene-2-carbonyl)phenol | HCID 13020505 | — |
| Product | HCID 22132807 | HCID 22132807 | 17.4% |
Reaction Steps
4-Chloro-6,7-dimethoxyquinoline (112 mg) and 4-hydroxyphenyl 2-thienyl ketone (102 mg) obtained in Example 39 were mixed and stirred at 160° C. for 40 minutes. The reaction mixture was purified in the same manner as described in Example 24 to obtain 34 mg of the title compound (yield: 17%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US06143764 |
|---|
| Source dataset | uspto-grants-2000_11 |
|---|
| ORD ID | ord-1d4d0d7b37634b689bee05cfc17604ae |
|---|
| Source note | uspto-grants-2000_11 |
|---|
