HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1857128Generated: November 2, 2026
4-Hydroxy-4'-chlorobenzophenone → HCID 22132804, compound
https://huagongshe.com/reaction/1857128
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 4-Hydroxy-4'-chlorobenzophenone | HCID 123504 | — |
| Reactant | 4-Chloro-6,7-dimethoxyquinoline | HCID 459610 | — |
| Product | HCID 22132804 | HCID 22132804 | 12.4% |
Reaction Steps
4-Chloro-6,7-dimethoxyquinoline (112 mg) and commercially available 4-chlorophenyl 4-hydroxyphenyl ketone (349 mg) were mixed and stirred at 180° C. for 20 minutes. The reaction mixture was purified by thin layer chromatography on silica gel eluting with chloroform/ethyl acetate (5/1) to obtain 26 mg of the title compound (yield: 12%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US06143764 |
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| Source dataset | uspto-grants-2000_11 |
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| ORD ID | ord-3e86ef713c2749bebb6541e063cb936e |
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| Source note | uspto-grants-2000_11 |
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