Water → 1,6-Hexanediol

HRID 1857297Notes

Reaction equation

HRID 1857297 reaction equation
[C:1]([O-:9])(=[O:8])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[Na+:10].[OH2:11]>>[C:1]([O-:9])(=[O:8])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[Na+:10].[CH2:6]([OH:11])[CH2:5][CH2:4][CH2:3][CH2:2][CH2:1][OH:9]

Participants

4

Reactant 2

HCID 962WaterHCID 517055Sodium Benzoate

Product 2

HCID 123741,6-HexanediolHCID 517055Sodium Benzoate

Procedure

The coolant composition of the present invention can be prepared by merely mixing the components (A), (B) and (C) each in a specified amount to give a uniform mixture. In an actual procedure, it is advantageous that sodium benzoate as the component (B) is first dissolved in water as the component (C) to give a uniform aqueous solution of sodium benzoate into which liquid 1,6-hexanediol prepared in advance by heating the solidified compound having a melting point of about 43° C. is added as the component (A) under agitation with a suitable stirrer. It is important in this case that entrainment of air into the mixture under agitation is minimized in order to avoid increase of the dissolved oxygen therein by adequately selecting the types of the stirrer blades and the velocity of stirrer revolution.

Workup

  1. customThe coolant composition of the present invention can be prepared
  2. customto give a uniform mixture

Sources & evidence

ORD record
ord-d02ba96f8d5d45619325ad623fc708e2
Source dataset
uspto-grants-2000_11
Patent number
US06146546

Reaction notes

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