Ethylene Glycol → HCID 22129439, compound

HRID 1857327Notes

Reaction equation

HRID 1857327 reaction equation
[CH3:1][C:2]1([CH3:16])[C:11]2[C:6](=[CH:7][CH:8]=[C:9](Br)[CH:10]=2)[C:5]([CH3:14])([CH3:13])[CH2:4][CH:3]1[CH3:15].C(N1CC[O:22][CH2:21][CH2:20]1)=O.C(O)[CH2:26][OH:27]>>[CH3:1][C:2]1([CH3:16])[C:11]2[C:6](=[CH:7][C:8]([C:21](=[O:22])[CH3:20])=[C:9]([CH:26]=[O:27])[CH:10]=2)[C:5]([CH3:14])([CH3:13])[CH2:4][CH:3]1[CH3:15]

Participants

4

Reactant 3

HCID 174Ethylene GlycolHCID 20417N-FormylmorpholineHCID 131722150HCID 131722150, compound

Product 1

HCID 22129439HCID 22129439, compound

Procedure

This compound was prepared according to Example 1 by acetylation of 1,1,2,4,4-Pentamethyl-7-bromo-1,2,3,4-tetrahydonaphtalene, ketalisation with ethyleneglycol, and Grignard-reaction with N-formylmorpholine.

Workup

  1. customThis compound was prepared

Sources & evidence

ORD record
ord-2f05db050e8640baafe677b63a351fe7
Source dataset
uspto-grants-2000_11
Patent number
US06147049

Reaction notes

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