HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Acid → HCID 367454, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | 4-Nitrobenzaldehyde | HCID 541 | — |
| Reactant | Piperidine | HCID 8082 | — |
| Reactant | Acetylacetone | HCID 31261 | — |
| Solvent | Isopropanol | HCID 3776 | — |
| Product | HCID 367454 | HCID 367454 | — |
Reaction Steps
30.2 g (0.2 mol) of 4-nitrobenzaldehyde and 30.0 g (0.3 mol) of acetylacetone are dissolved in 200 ml of isopropanol and treated with 1.2 ml of piperidine and 1 ml of glacial acetic acid. The mixture is warmed in a water bath until a clear solution is formed and then stirred at RT for 4 h. The product precipitates and is filtered off with suction.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06147087 |
| Source dataset | uspto-grants-2000_11 |
| ORD ID | ord-a570f78df2fc4530abca2a69c8ff7e55 |
| Source note | uspto-grants-2000_11 |