HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 53657430, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 2-Chlorobenzylamine | HCID 66648 | — |
| Reactant | HCID 178512266 | HCID 178512266 | — |
| Product | HCID 53657430 | HCID 53657430 | 72% |
Reaction Steps
By following a procedure analogous to the one described above in Example 1b, N-(3,5-bis(trifluoromethyl)phenyl)-N'-cyano-O-phenylisourea (0.300 g, 0.8 mmol) was treated with triethylamine (0.123 ml, 0.88 mmol) and 2-chlorobenzylamine (0.107 ml, 0.88 mmol) to give the title compound as a syrup. Yield 72% (0.234 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06147098 |
| Source dataset | uspto-grants-2000_11 |
| ORD ID | ord-696c83acdc114f01be9e27ddfeb07148 |
| Source note | uspto-grants-2000_11 |