HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 15484977, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | 4-Bromophenyl isocyanate | HCID 75609 | — |
| Reactant | Cyclopentanesulfonamide | HCID 4645983 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 15484977 | HCID 15484977 | 83.2% |
Reaction Steps
The general method of procedure A was followed with cyclopentanesulfonamide (3 g), acetone (100 ml), 1N sodium hydroxide (21 ml), and 4-bromophenyl isocyanate (3.7 g) dissolved in acetone (50 ml). After two hours, 1N HCl (21 ml) was added. The resulting precipitate was collected, washed with water and dried at 60° C. under vacuum to provide 5.4 g of product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06147115 |
| Source dataset | uspto-grants-2000_11 |
| ORD ID | ord-2a2a84b0c2194bf196738fcc6bb7b1e7 |
| Source note | uspto-grants-2000_11 |