HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 15484978, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | 3,4-Dichlorophenyl isocyanate | HCID 7607 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | Cyclopentanesulfonamide | HCID 4645983 | — |
| Solvent | Acetone | HCID 180 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 15484978 | HCID 15484978 | 85.2% |
Reaction Steps
The general method of procedure A was followed with cyclopentanesulfonamide (3 g), acetone (200 ml), 1N sodium hydroxide (20 ml), and 3,4-dichlorophenyl isocyanate (3.6 g) dissolved in acetone (50 ml). After two hours, 1N HCl (20 ml) was added and the resulting solid diluted with water and collected. After drying at 65° C., 5.5 g of solid product were obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06147115 |
| Source dataset | uspto-grants-2000_11 |
| ORD ID | ord-83b3f892b59f493092b1d9beb4ac4ce3 |
| Source note | uspto-grants-2000_11 |