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HRID1857885

反应详情

EQUATION

反应方程式

HRID 1857885 的结构方程式

REACTANTS

反应物

2
结构：O=Cc1cc(Br)c[nH]1
HCID599627

4-Bromo-1H-pyrrole-2-carbaldehyde

C5H4BrNO

结构：Cc1cc2c(cc1B(O)O)C(C)(C)CCC2(C)C
HCID10037535

(3,5,5,8,8-Pentamethyl-5,6,7,8-tetrahydronaphthalen-2-yl)boronic acid

C15H23BO2

PRODUCTS

生成物

1
结构：Cc1cc2c(cc1-c1c[nH]c(C=O)c1)C(C)(C)CCC2(C)C
HCID22131507

未命名化合物

PROCEDURE

实验过程

In a similar manner to Example 3(b), by reaction of 2.47 g (10 mmol) of 3,5,5,8,8-pentamethyl-5,6,7,8-tetrahydro-2-naphthylboronic acid with 1.5 g (8.4 mmol) of 4-bromo-2-pyrrolecarboxaldehyde, 950 mg (38.5%) of the expected aldehyde are obtained, with a melting point of 128-9° C.

WORKUP

后处理

  1. customare obtained, with a melting point of 128-9° C.