Fumaric Acid → HCID 21954893, compound

HRID 1857929Notes

Reaction equation

HRID 1857929 reaction equation
[C:1]([OH:8])(=[O:7])/[CH:2]=[CH:3]/[C:4]([OH:6])=[O:5]>C(O)(C)C>[OH2:5].[C:1]([OH:8])(=[O:7])/[CH:2]=[CH:3]/[C:4]([OH:6])=[O:5]

Participants

3

Reactant 1

HCID 444972Fumaric Acid

Product 1

HCID 21954893HCID 21954893, compoundYield 568.9%

Reagents, catalysts & solvents 1

HCID 3776IsopropanolSolvent

Procedure

To an ice-cooled solution of compound 2 (4.17 g) in isopropanol (80 ml) was added fumaric acid (1.26 g), and the mixture was stirred at room temperature for 8 hours. The resulting crystals were collected by filtration, and dried under reduced pressure to give fumarate hydrate (4.14 g) of compound 2 as white crystals.

Workup

  1. filtrationThe resulting crystals were collected by filtration
  2. customdried under reduced pressure

Sources & evidence

ORD record
ord-624809f77cf54b2ebdc0fc92818c1d66
Source dataset
uspto-grants-2000_11
Patent number
US06150355

Reaction notes

Loading…