HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dicyandiamide → HCID 9927584, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dicyandiamide | HCID 10005 | — |
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | 1-(Diphenylmethyl)azetidine-3-carbonitrile | HCID 2779290 | — |
| Solvent | Water | HCID 962 | — |
| Solvent | 2-Methoxyethanol | HCID 8019 | — |
| Product | HCID 9927584 | HCID 9927584 | — |
Reaction Steps
A solution of 1-(diphenylmethyl)-3-azetidinecarbonitrile (500 mg, 2.01 mmol), dicyandiamide (220 mg, 2.62 mmol) and KOH (34 mg, 0.604 mmol) in 2-methoxyethanol (10 mL) was heated at reflux for 4 hours, diluted with water, and cooled to room temperature. The precipitate was rinsed with water and dried under vacuum to provide the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06150362 |
| Source dataset | uspto-grants-2000_11 |
| ORD ID | ord-3e24e78bd94f4eb29b322f54245185d6 |
| Source note | uspto-grants-2000_11 |