Potassium Hydroxide → 6-(1,4-Dioxa-8-azaspiro[4,5]dec-8-yl)-1,3,5-triazine-2,4-diamine

Beteiligte Stoffe

Rolle	Name	HCID	Einwaage
Edukt	Potassium Hydroxide	HCID 14797	—
Edukt	1,3,5-Triazine-2,4-diamine, 6-chloro-	HCID 18831	—
Edukt	1,4-Dioxa-8-azaspiro(4.5)decane	HCID 67435	—
Lösungsmittel	Ethanol	HCID 702	—
Lösungsmittel	Water	HCID 962	—
Lösungsmittel	1,4-Dioxane	HCID 31275	—
Produkt	6-(1,4-Dioxa-8-azaspiro[4,5]dec-8-yl)-1,3,5-triazine-2,4-diamine	HCID 9816436	—

Reaktionsschritte

A mixture of 2,4-diamino-6-chloro-1,3,5-triazine (2 g, 14 mmol), 1,4-dioxa-8-azaspiro[4.5]decane (3 g, 21 mmol), and KOH (100 mg, 1.8 mmol) in dioxane (10 mL) and ethanol (40 mL) was heated at reflux overnight, diluted with water, and filtered. The precipitate was rinsed with water and dried under vacuum to provide the title compound.

Herkunft & Nachweise

DOI	10.6084/m9.figshare.5104873.v1
Patentnummer	US06150362
Quelldatensatz	uspto-grants-2000_11
ORD ID	ord-698fd8cabfbe49b284e7f0777a4faaf4
Quellennotiz	uspto-grants-2000_11