HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Phosphate, Dibasic → HCID 9881623, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Phosphate, Dibasic | HCID 24450 | — |
| Reactant | N-BOC-ethylenediamine | HCID 187201 | — |
| Reactant | 2-Amino-5-bromo-1,3,4-thiadiazole | HCID 3650883 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 9881623 | HCID 9881623 | 79.4% |
Reaction Steps
A mixture of 5-bromo-1,3,4-thiadiazol-2-ylamine (5.40 g), K2HPO4 (7.84 g), and Boc-ethylenediamine (9.6 g) in 20 ml of DMF is stirred at ambient temperature for 18 hours. The solid paste obtained is recrystallized from 100 ml of acetonitrile and 100 ml of water to provide 6.18 g (79%) of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06150385 |
| Source dataset | uspto-grants-2000_11 |
| ORD ID | ord-9b96220e0f0a44ddbe0100e42b9aadf4 |
| Source note | uspto-grants-2000_11 |