Potassium Nitrate → HCID 22125760, compound

HRID 1858039Notes

Reaction equation

HRID 1858039 reaction equation
[OH:1][C:2]1[C:3]([O:17][CH3:18])=[CH:4][C:5]([N+:14]([O-:16])=[O:15])=[C:6]([CH2:8][CH2:9][CH2:10][C:11]([OH:13])=[O:12])[CH:7]=1.[N+:19]([O-])([O-:21])=[O:20].[K+]>S(=O)(=O)(O)O>[N+:19]([C:7]1[C:2]([OH:1])=[C:3]([O:17][CH3:18])[CH:4]=[C:5]([N+:14]([O-:16])=[O:15])[C:6]=1[CH2:8][CH2:9][CH2:10][C:11]([OH:13])=[O:12])([O-:21])=[O:20]

Participants

4

Reactant 2

HCID 24434Potassium NitrateHCID 22125744HCID 22125744, compound

Product 1

HCID 22125760HCID 22125760, compound

Reagents, catalysts & solvents 1

HCID 1118Sulfuric AcidSolvent

Conditions

Temperature
-15 °C

Procedure

The product from Example 1 (0.77 g) was dissolved in concentrated sulfuric acid and cooled to -15° C. Potassium nitrate (0.31 g) was gradually added to this solution while maintaining the reaction temperature between -15 and -10° C. The resultant mixture was stirred at -15° C. for half an hour and then poured into ice. The solid was washed with water and dried.

Workup

  1. temperaturewhile maintaining the reaction temperature between -15 and -10° C
  2. additionpoured into ice
  3. washThe solid was washed with water
  4. customdried

Sources & evidence

ORD record
ord-f28821e4a12f4255874a9350307e765e
Source dataset
uspto-grants-2000_11
Patent number
US06150412

Reaction notes

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