Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Potassium Nitrate | HCID 24434 | — |
| Reactant | HCID 22125744 | HCID 22125744 | — |
| Solvent | Sulfuric Acid | HCID 1118 | — |
| Product | HCID 22125760 | HCID 22125760 | — |
Reaction Steps
The product from Example 1 (0.77 g) was dissolved in concentrated sulfuric acid and cooled to -15° C. Potassium nitrate (0.31 g) was gradually added to this solution while maintaining the reaction temperature between -15 and -10° C. The resultant mixture was stirred at -15° C. for half an hour and then poured into ice. The solid was washed with water and dried.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US06150412 |
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| Source dataset | uspto-grants-2000_11 |
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| ORD ID | ord-f28821e4a12f4255874a9350307e765e |
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| Source note | uspto-grants-2000_11 |
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