HuagongsheHuagongshe Chemistry Print Report · For research reference only
Nitric Acid → 6-(4,5-Dimethoxy-2-nitrophenyl)hexanoic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Nitric Acid | HCID 944 | — |
| Reactant | 6-(3,4-dimethoxyphenyl)hexanoic Acid | HCID 4577343 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | 6-(4,5-Dimethoxy-2-nitrophenyl)hexanoic acid | HCID 22125750 | — |
Reaction Steps
To a solution of 6-(3,4-dimethoxyphenyl)hexanoic acid (2.7 g) in acetic acid (10 ml) was added nitric acid (5.4 ml of a 2 M solution in acetic acid) and the mixture stirred at room temperature for one hour. The mixture was evaporated and the product used as such for the next step. Yield: 3.2 g.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06150412 |
| Source dataset | uspto-grants-2000_11 |
| ORD ID | ord-9e398f8181fd479ea2eab38954b815c7 |
| Source note | uspto-grants-2000_11 |