Methyl 4-ethynylbenzoate → HCID 54554152, compound

Participants

Reaction Steps

In a similar manner to that of Example 1(e), by reaction of 3.69 g (11.0 mmol) of 2-((E)-2-iodovinyl)-5,4'-dimethylbiphenyl obtained in Example 13(f) with 1.60 g (10.0 mmol) of methyl 4-ethynylbenzoate, 1.00 g (27%) of the expected compound is obtained in the form of a white powder with a melting point of 123-125° C.

Provenance & Evidence