Methyl 4-ethynylbenzoate → HCID 54116665, compound

Participants

Reaction Steps

In a similar manner to that of Example 1(e), by reaction of 2.40 g (7.0 mmol) of 2-((E)-2-iodovinyl)-4'-chlorobiphenyl obtained in Example 23(b) with 1.03 g (6.4 mmol) of methyl 4-ethynylbenzoate, 970 mg (41%) of the expected compound are obtained in the form of a pale yellow solid with a melting point of 135° C.

Provenance & Evidence