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Hydroquinone → tert-Butyl peroxybenzoate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Hydroquinone | HCID 785 | — |
| 反応物 | N,N-Dimethylaniline | HCID 949 | — |
| 反応物 | Dicumyl peroxide | HCID 6641 | — |
| 反応物 | Diethylene glycol diacrylate | HCID 19996 | — |
| 反応物 | Methyl ethyl ketone peroxide | HCID 3672772 | — |
| 反応物 | Alumina | HCID 9989226 | — |
| 反応物 | Sodium Methoxide | HCID 10942334 | — |
| 溶媒 | Toluene | HCID 1140 | — |
| 溶媒 | Dichloromethane | HCID 6344 | — |
| 生成物 | tert-Butyl peroxybenzoate | HCID 11966 | — |
反応手順
Sodium methoxide (NaOCH3), toluene (anhydrous), dichloromethane, hexanes, activated neutral aluminum oxide (60 to 50 mesh), hydroquinone, methyl ethyl ketone peroxide, dimethylaniline, dicumylperoxide, diethylene glycol diacrylate, and tert-butylperoxybenzoate were obtained from commercial sources and used as received.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06150429 |
| 出典データセット | uspto-grants-2000_11 |
| ORD ID | ord-1b265212be2f48a2b206a49a2742bb59 |
| 出典メモ | uspto-grants-2000_11 |