Methane → HCID 15385774, compound

Participants

Reaction Steps

4,5α-epoxy-6α-((5-methoxycarbonyl-valeryl)-oxy)-3-methoxymethoxy-17-methyl-morphinan-7-ene (0.48 g, 1.02 mmol) was dissolved in MeOH (30 ml), mixed with 10% Pd on 0.35 g of activated charcoal and then agitated for 2 hours at ambient temperature under H2 (1 bar over pressure). The catalyst was illuminated by filtering through a filter compound and the filtrate was concentrated by rotary evaporation.

Provenance & Evidence