HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 15351904, compound → HCID 15385697, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 15351904 | HCID 15351904 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 15385697 | HCID 15385697 | — |
Reaction Steps
4,5α-Epoxy-3-methoxymethoxy-17-methyl-6α-((2-pyridyl)-oxy)-morphinan-7-ene (1.0 g. 2.46 mmol) is dissolved in MeOH (40 ml), mixed with 10% Pd unactivated charcoal 800 mg and then agitated at RT under H2 (1 bar over pressure) for 2 hours. The catalyst is eliminated by filtering over a filter compound and a filtrate is concentrated by rotary evaporation.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06150524 |
| Source dataset | uspto-grants-2000_11 |
| ORD ID | ord-22a0e1bda73c4640bf1c4bad5e01b6cc |
| Source note | uspto-grants-2000_11 |