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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1858357Generated: November 1, 2026

HCID 15351904, compound → HCID 15385697, compound

https://huagongshe.com/reaction/1858357

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 15351904HCID 15351904—
CatalystPalladiumHCID 23938—
SolventMethanolHCID 887—
ProductHCID 15385697HCID 15385697—

Reaction Steps

4,5α-Epoxy-3-methoxymethoxy-17-methyl-6α-((2-pyridyl)-oxy)-morphinan-7-ene (1.0 g. 2.46 mmol) is dissolved in MeOH (40 ml), mixed with 10% Pd unactivated charcoal 800 mg and then agitated at RT under H2 (1 bar over pressure) for 2 hours. The catalyst is eliminated by filtering over a filter compound and a filtrate is concentrated by rotary evaporation.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06150524
Source datasetuspto-grants-2000_11
ORD IDord-22a0e1bda73c4640bf1c4bad5e01b6cc
Source noteuspto-grants-2000_11