Trichlorosilane → HCID 22129125, compound

Participants

Reaction Steps

A one-liter autoclave equipped with a stirrer was charged in a nitrogen atmosphere with 50 grams (0.40 mol) of 1-tert-butylcyclopentene, 108 grams (0.80 mol) of trichlorosilane and 20 grams (82 mmol) of 1,1'-azobis(cyclohexane-1-carbonitrle) and the mixture was reacted at a temperature of 130° C. for 3 days. The resulting reaction mixture was purified by distillation thereby obtaining 62 grams (0.24 mol) of 2-tert-butylcyclopentyltrichlorosilane. The structure of the resulting product was identified by 1H-NMR.

Provenance & Evidence