HuagongsheHuagongshe Chemistry Print Report · For research reference only
(2S,5R)-1-Boc-2,5-dimethylpiperazine → HCID 70272419, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (2S,5R)-1-Boc-2,5-dimethylpiperazine | HCID 11745988 | — |
| Reactant | 4-Methylisoquinoline-5-sulfonyl chloride | HCID 15487110 | — |
| Product | HCID 70272419 | HCID 70272419 | 82.8% |
Reaction Steps
Using 0.34 g of trans-1-(tert-butoxycarbonyl)-2,5-dimethylpiperazine and 0.64 g of 5-chlorosulfonyl-4-methylisoquinoline, the procedure of Example 1 was otherwise repeated to provide 0.43 g of the objective compound (white crystals).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06153608 |
| Source dataset | uspto-grants-2000_11 |
| ORD ID | ord-60acfc09b9c24031aced920decad53ae |
| Source note | uspto-grants-2000_11 |