HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Methylisoquinoline-5-sulfonyl chloride → HCID 21948557, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Methylisoquinoline-5-sulfonyl chloride | HCID 15487110 | — |
| Reactant | 5-Methyl-1,4-diazepane | HCID 18545617 | — |
| Product | HCID 21948557 | HCID 21948557 | 77% |
Reaction Steps
Using 0.29 g of hexahydro-5-methyl-1H-1,4-diazepine synthesized in accordance with U.S. Pat. No. 3,040,029 and 0.48 g of 5-chlorosulfonyl-4-methylisoquinoline, the procedure of Example 1 was otherwise repeated to provide 0.3 g of the objective compound (white crystals).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06153608 |
| Source dataset | uspto-grants-2000_11 |
| ORD ID | ord-9f08fe99771749618caf129b1f9c182e |
| Source note | uspto-grants-2000_11 |